Synthesis and magnetic properties of magnetic-improved SBA 15 mesoporous composites by nanoparticles
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Abstract
The nano-Co3O4 and nano-CoFe2O4 modified SBA-15 magnetic mesoporous, Co3O4 /SBA-15 and CoFe2O4/SBA-15 composites were prepared by immersion method. The microstructure and magnetic properties of the composites were analyzed by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM) and vibrating sample magnetometer (VSM). All results indicate that Co3O4 and CoFe2O4 nanoparticles exist in the mesopores of SBA-15, which can improve the magnetic properties of the SBA-15 nanocomposites. The study reveals that the magnetic properties of SBA-15 nanocomposites are attributed to the doped magnetic nanoparticles. And the magnetic properties are improved with the content of Co3O4 and CoFe2O4 nanoparticles, in which the coercivity reaches the maximum of 400 Oe and the saturation magnetization is 9emu/g.
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