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MXene基复合材料的制备及其在钠、钾离子电池中的应用

刘纳 王雅婷 修石健 李仁哲 权波

刘纳, 王雅婷, 修石健, 等. MXene基复合材料的制备及其在钠、钾离子电池中的应用[J]. 复合材料学报, 2023, 42(0): 1-14.
引用本文: 刘纳, 王雅婷, 修石健, 等. MXene基复合材料的制备及其在钠、钾离子电池中的应用[J]. 复合材料学报, 2023, 42(0): 1-14.
LIU Na, WANG Ya-ting, XIU Shi-jian, et al. Preparation of MXene-based composites and their applications in sodium and potassium-ion batteries[J]. Acta Materiae Compositae Sinica.
Citation: LIU Na, WANG Ya-ting, XIU Shi-jian, et al. Preparation of MXene-based composites and their applications in sodium and potassium-ion batteries[J]. Acta Materiae Compositae Sinica.

MXene基复合材料的制备及其在钠、钾离子电池中的应用

基金项目: 吉林省教育厅科学技术项目(JJKH20191122KJ)
详细信息
    通讯作者:

    权波,博士,教授,研究方向为无机材料、功能复合材料 E-mail: quanbo@ybu.edu.cn

  • 中图分类号: TM912;TB30;TB332

Preparation of MXene-based composites and their applications in sodium and potassium-ion batteries

Funds: Science and Technology Project of Jilin Provincial Department of Education (JJKH20191122KJ)
  • 摘要: MXene及其复合材料在二次电池领域得到了广泛的应用。MXene作为一种新型二维过渡金属碳化物层状材料,它的电导率极高,比表面积极大,层状结构独特,表面活性位点众多,离子传输路径极短,力学性能卓越,因此,MXene已经被广泛地应用于储能、吸附、催化等各个领域。以MXene基构建复合材料不仅可以提高导电性,缓解体积膨胀,反过来还可以抑制MXene堆叠,获得更好的电化学性能。本文综述了MXene含氟和无氟的合成方法,分析了MXene及其复合材料在钠、钾离子电池中的应用及性能。最后,阐述了MXene及其复合材料的挑战和前景。

     

  • 图  1  (a) Ti3C2Tx 与HF反应后Al原子被OH取代并在甲醇中超声处理后氢键断裂和纳米片分离示意图[20]。(b) HF处理后样品的结构表征图像[20]。(c)从Ti3AlC2到Ti3C2Tx的蚀刻示意图[23]。(d) Hf蚀刻Ti3C2Tx的结构表征图[23]。(e)用HF或LiF-HCL刻蚀Ti3AlC2和Ti3C2Tx的XRD谱图[23]

    Figure  1.  (a) Schematic diagram of hydrogen bond cleavage and nanosheet separation after the reaction of Ti3C2Tx with HF after the Al atom is replaced by OH and sonicated in methanol[20]. (b) Structural characterization image of the HF-treated sample[20]. (c) Schematic diagram of etching from Ti3AlC2 to Ti3C2Tx[23]. (d) Structural characterization of Hf-etched Ti3C2Tx[23]. (e) XRD spectra of Ti3AlC2 and Ti3C2Tx etched with HF or LiF-HCL[23].

    图  2  (a) Ti3AlC2与NaOH水溶液在不同条件下的反应[35]。(b) Ti4AlN3在550℃氩气条件下进行熔盐处理合成Ti4N3Tx的示意图,然后用TBAOH将多层MXene分层[41]

    Figure  2.  (a) The reaction between Ti3AlC2 and NaOH water solution under different conditions[35]. (b) Schematic illustration of the synthesis of Ti4N3Tx by molten salt treatment of Ti4AlN3 at 550°C under Ar, followed by delamination of the multilayered MXene by TBAOH[41]

    图  3  (a)中空MXene球体和三维大孔MXene框架的结构示意图[65]。(b) Sb2O3/MXene(Ti3C2Tx)的制备工艺示意图[67]。(c)真空辅助过滤法制备MXene/SnS2复合材料示意图[71]。(d)三维f-Ti3C2/NiCo2Se4体系结构的合成过程示意图[76]

    Figure  3.  (a) Schematic showing the construction of hollow MXene spheres and 3D macroporous [65]. (b) Schematic illustration of the preparation process for Sb2O3/MXene(Ti3C2Tx)[67]. (c) Schematic illustration of the preparation of MXene/SnS2 composite by vacuum-assisted filtration[71]. (d) Schematic illustration of the synthetic process of the 3D f-Ti3C2/NiCo2Se4 architectures[76].

    图  4  (a) Te-SnS2/MXene结构的制备示意图[88]. (b) VSe2/MXene@C的合成示意图,VSe2/MXene@C中K+或电子的扩散路径,VSe2/MXene@C的结构模型[84]

    Figure  4.  :(a) Schematic of the preparation of Te-SnS2/MXene superstructure[88]. (b) Schematic preparation of the synthesis of VSe2/MXene@C, paths for diffusion of K+ or electrons in the VSe2/MXene@C, structural model of VSe2/MXene@C[84].

    表  1  MXene基材料在钠离子电池和钾离子电池中的最新性能比较

    Table  1.   Comparison of the latest performance of MXene-based materials in sodium-ion and potassium-ion batteries

    MXene and its composite materials are used in sodium-ion batteries MXene and its composites are used in potassium-ion batteries
    Materials Rate performance and cycle performance Ref. Materials Rate performance and cycle performance Ref.
    f-Ti3C2TxDMSO 267 mAh·g−1 at 0.1 A·g−1;76 mAh·g–1 after 1500 cycles at 1 A·g−1 [49] S-Ti3C2TX 101 mAh·g−1 at 0.1 A·g−1;41 mAh·g−1 after 2000 cycles at 0.5 A·g−1 [72]
    Sulfur-doped multilayer Ti3C2Tx 121.3 mAh·g−1 at 2 A·g−1;183.2 mAh·g−1 after 100 cycles at 0.1 A·g−1 [54] MXene@CNTs 250 mAh·g−1 at 0.05 A·g−1 [73]
    O-Ti3C2Tx 153 mAh·g−1 after 2500 cycles at 1 A·g−1 [56] CSs@ Ti3C2 195.8 mAh g−1 after 200 cycles at 0.1 A g−1 [74]
    Alkalizing three-dimensional Ti3C2 168 mAh·g−1 at 0.02 A·g−1 [57] MoSe2/MXene@C 355 mAh·g−1 after 100 cycles at 0.2 A·g−1 [75]
    p-Ti3C2Tx 166 mAh·g−1 at 1 A·g−1;124 mAh·g−1 at 10 A·g−1;24 mAh·g−1 at 100 A·g−1;
    1000 cycles at 1 A·g−1
    [59] Fe2O3@carbon/
    MXene
    169 mAh g−1 at 5 A·g−1;410 mAh g−1 after 200 cycles at 0.1 A·g−1 [76]
    VO2/MXene 280.9 mAh·g−1 after 200 cycles at 0.1 A·g−1 [61] VSe2/MXene@C 138.7 mAh·g−1 after 500 cycles at 1 A·g−1 [77]
    TiO2/Ti3C2 237.8 mAh·g−1 at 0.1 A·g−1 [62] Ti3C2TX/MnS 127 mAh·g−1 after 2000 cycles at 0.2 A·g−1 [78]
    MXene/SnS2 322 mAh·g−1 after 200 cycles at 0.1 A·g−1 [64] Te-SnS2/MXene 343.2 mAh·g−1 after 50 cycles at 0.2 A·g−1;165.8 mAh·g−1 after 5000 cycles at 10 A·g−1 [81]
    Ti3C2Tx/CoS2@NC 200.6 mAh·g−1 after 1500 cycles at 2 A·g−1 [67] CAS-Ti3C2 496.7 mAh·g−1 after 200 cycles at 0.1 A·g−1 [82]
    MoSe2/MXene 490 mAh·g−1 after 200 cycles at 1 A·g−1 [68] (CoS NP@NHC)@
    MXene
    210 mAh·g−1 after 500 cycles at 2 A·g−1 [84]
    Notes:f—Fewer layers; DMSO—Dimethyl sulfoxide; CNTs—Carbon nanotubes; CS—Carbon balls; p—Porous anisotropic structure; CAS—Cu12Sb4S13 quantum dots; NC—Nitrogen-doped carbon; NP—Nanoparticles
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出版历程
  • 收稿日期:  2023-09-27
  • 修回日期:  2023-11-15
  • 录用日期:  2023-12-06
  • 网络出版日期:  2023-12-28

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