Research progress in the preparation and application of functional materials based on inverse opal structure in water treatment fields
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摘要: 反蛋白结构(IO)是光子晶体的一种典型的空间结构构型。IO除了具有相互连通、高度规整有序的均孔结构外，还具有光子晶体的慢光效应、多次散射效应和放大光子吸收、发射的特性等。近年来，对IO的应用包括均孔膜、光子墨水、电池电极、传感器等。本文首先简述了IO的构建策略，分为“三步法”和“两步法”。进而详细总结了IO在水处理领域的研究进展，包括过滤筛分、高效吸附、催化降解、水质检测4个方面。最后，对IO材料在水处理领域中现有的局限性和未来的发展趋势进行了阐述和展望。Abstract: The inverse opal structure (IO) is a typical spatial structure of photonic crystals. In addition to the interconnected, highly regular, and orderly homoporous structure, IO also has the properties of photonic crystals, including the slow light effect, multiple scattering effects, amplified photon absorption and emission characteristics. In recent years, applications for IO have included homoporous membranes, photonic inks, battery electrodes, sensors, etc. In this paper, we first briefly describe the construction strategy of IO, which is divided into the "three-step method" and "two-step method". Then, the research progress of IO in water treatment fields was summarized in detail, including filtration and screening, efficient adsorption, catalytic degradation, and water quality detection. Finally, the existing limitations and future development trends of IO materials in water treatment fields were elaborated and prospected.
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图 4 三步法(a)、两步法(b)制备反蛋白石结构的示意图
Figure 4. Preparation of inverse opal films by the three-step method (a) and the two-step method (b)
图 8 (a) 胶体晶体模板中SiO2颗粒直径与IO膜中“较小”孔径之间的关系；(b) 使用375 nm、440 nm和835 nm SiO2颗粒制备的IO膜的纯水通量[30]
Figure 8. (a) Relationship between the diameter of SiO2 particles in the colloidal crystal template and the "smaller" pore size in the IO film; (b) Deionized water fluxes for membranes fabricated using 375 nm, 440 nm and 835 nm silica particles[30]
图 13 (a) 黑磷纳米粒子(BPQDs)-IO TiO2的构筑和光催化性能[115]；(b) 引入嵌段聚合物制备分级3D介孔TiO2 IO (3D-HPT)及对染料的催化降解性能[16]
NHE—Normal hydrogen electrode; P25—Commercially P25 TiO2 powders; kapp—The apparent kinetic constants; 3DOM—Three-dimensional macro-porous; P123—Pluronic P123 (PEG-PPG-PEG), a versatile tri-block copolymer; MO—Methylorange; MB—Methylene blue; RhB—Rhodamine B; X3B—Reactive brilliant red; 3D-T—Conventional three-dimensional macro-porous TiO2; 3D-HPT—Three-dimensional hierarchical mesoporous structures of TiO2
Figure 13. (a) Construction and photocatalytic performance of black phosphorus nanoparticles (BPQDs)-IO TiO2[115]; (b) Preparation of the hierarchical 3D macro-porous TiO2 IO by introducing block polymers (3D-HPT) and its catalytic degradation performance of dyes[16]
图 14 (a) 氧化石墨烯纳米胶粒表面功能化的TiO2反蛋白石膜 (nano GO-PC)[17]；(b) 空心半球形结构Si掺杂TiO2 (HHS-Si/TiO2)的构筑策略和催化性能[35]
TiO2 IO are named as PC220, PC350, PC425 and PC510, according to the diameter of the PS colloidal sphere; PCmix stands for the disordered TiO2 IO; P25 denote the commercially P25 TiO2 powders; k—The apparent rate constants; MB—Methylene blue; GO—Graphene oxide
Figure 14. (a) Graphene oxide nanocolloids (nano GO) surface-functionalized TiO2 IO[17]; (b) Construction strategy and catalytic performance of the hollow hemispherical structured Si-doped TiO2 (HHS-Si/TiO2)[35]
图 15 反蛋白石结构的S型异质结−Ag/ZnO/CeO2 IO的构建策略及对染料的催化降解性能[113]
SM—Styrene; AA—Methacrylic acid; KPS—Potassium persulfate; Ag NPs—Ag nanoparticles; Selt—Blank experiments; C0, C—Initial (t = 0) and residual (t time) concentrations of RhB
Figure 15. Construction strategy and catalytic degradation performance of dyes of S-type heterojunction—Ag/ZnO/CeO2 IO[113]
图 16 (a) 漆酶固定的反蛋白石水凝胶(LAC@MPEGDA@CS@IOH)的制备[25]；(b)氧化锌负载苯胺黑-聚偏氟乙烯反蛋白石(ZnO/AB-PVDF IO)的制备策略及光催化性能的增强[112]
Figure 16. (a) Preparation of immobilization of laccase on the poly(ethylene glycol) diacrylate (PEGDA)–chitosan (CS) inverse opal hydrogel (LAC@MPEGDA@CS@IOH) and their catalytic degradation performance of bisphenol contaminants[25]; (b) Preparation strategy and photocatalytic performance of ZnO/the aniline black-poly(vinylidene fluoride) (AB-PVDF) IO[112]
图 17 (a)合成反蛋白石金属有机框架(IO MOF)的通用策略和对4-硝基苯酚(4-NP)的水解速率[20]；(b)基于多巴胺层原位生长银纳米粒子(Ag NPs)的IO膜[18]
DMF—Dimethyl fumarate; PS—Polystyrene; PVP—Polyvinyl pyrrolidone; PCN-777—A zeo type mesoporous Zr-containing MOF; MOD-808, PCN-777, UN-1200, NU-1000, UiO-6—A series of inverse opal zirconium-based MOFs with intrinsic micro- and/or meso-pores; IO+MOFs—MOFs material with inverse opal structure; ZrO2—Commercial ZrO2 powder; Active C—Activated carbon
Figure 17. (a) General strategy for the synthesis of inverse opal metal-organic frameworks (IO MOFs) and hydrolysis of 4-nitrophenol (4-NP) [20]; (b) IO membranes based on dopamine layer-based in-situ growth of Ag nanoparticles (Ag NPs) [18]
图 19 (a) 用于水中Hg(II)浓度可视化检测的反蛋白石聚合光子晶体 (IOPPC) [40]；(b) 用于Cr(VI)检测的壳聚糖反蛋白石颗粒(IOP)[119]；(c) 用于水中乙醇浓度检测的新型聚醚砜/聚丙烯酸反蛋白石光子晶体[121]
CS—Chitosan; PEGDA—Polyethylene glycol diacrylate; c[Cr(VI)]—The concentration of Cr(VI); t—Response time; R2—Coefficient of determination; K=(λ1−λion)/(λ1−λ0), where λ0 is the original peak position of the IOPPCs, λ1 is the peak position of the IOPPCs immersed in the solution of urea with urease, λion is the peak position of the IOPPCs after adding various metal ions; IOPPCs means the pH-sensitive inverse opal polymeric photonic crystals
Figure 19. (a) Inverse opal polymeric photonic crystals (IOPPCs) for visual detection of Hg(II) concentrations in water[40]; (b) Chitosan inverse opal particles (IOPs) for Cr(VI) detection[119]; (c) Novel polyethersulfone/polyacrylic acid inverse opal photonic crystals for the detection of ethanol concentration in water[121]
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