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Fe3O4纳米材料在印染废水处理中的研究进展

宋杰枫 李皓天 聂子聪 李心如 肖远淑

宋杰枫, 李皓天, 聂子聪, 等. Fe3O4纳米材料在印染废水处理中的研究进展[J]. 复合材料学报, 2024, 43(0): 1-13.
引用本文: 宋杰枫, 李皓天, 聂子聪, 等. Fe3O4纳米材料在印染废水处理中的研究进展[J]. 复合材料学报, 2024, 43(0): 1-13.
SONG Jiefeng, LI Haotian, NIE Zicong, et al. Preparation and modification of Fe3O4 nanomaterials and their application in printing and dyeing wastewater treatment[J]. Acta Materiae Compositae Sinica.
Citation: SONG Jiefeng, LI Haotian, NIE Zicong, et al. Preparation and modification of Fe3O4 nanomaterials and their application in printing and dyeing wastewater treatment[J]. Acta Materiae Compositae Sinica.

Fe3O4纳米材料在印染废水处理中的研究进展

基金项目: 新疆维吾尔自治区重点研发任务专项(2022B01045-4);新疆维吾尔自治区高校基本科研业务费科研项目(XJEDU2022P005)、(XJEDU2024P028);2023年国家级大学生创新训练计划项目(202310755020)
详细信息
    通讯作者:

    肖远淑,讲师,硕士研究生,研究方向为清洁染整与功能纺织品开发。 E-mail:xiaoyuanshu122@xju.edu.cn

  • 中图分类号: TB333

Preparation and modification of Fe3O4 nanomaterials and their application in printing and dyeing wastewater treatment

Funds: The Key Research and Development Special Task Project of Xinjiang (No. 2022B01045-4); Xinjiang Uygur Autonomous Region Colleges and Universities Basic Research Operating Expenses Scientific Research Projects (No.XJEDU2022P005)、(No.XJEDU2024P028);2023 National Innovative Training Program for College Students Project (202310755020)
  • 摘要: 印染废水成分复杂,其中存在大量的有机染料和其他污染物,对环境和人体健康造成极大危害。传统的废水处理方法往往难以有效去除这些有机污染物,近年来,人们开始关注利用纳米材料来解决这一问题。Fe3O4纳米材料因具有磁性、生物相容性和光学特性等优异性能,已逐渐成为废水处理中具有巨大应用前景的新型材料。本文阐述了利用物理、化学、生物等方法制备出高质量Fe3O4纳米材料的过程,介绍了利用有机材料、无机材料、框架材料等对其进行改性的方法,用以解决材料易团聚的问题并提高其稳定性。综述了Fe3O4纳米材料在印染废水处理领域的最新应用研究进展,最后,对Fe3O4纳米材料的制备方法和应用研究进行了讨论,旨在为促进Fe3O4纳米材料的推广应用提供理论参考。

     

  • 图  1  不同制备方法得到的Fe3O4纳米材料的SEM或TEM图像(a)机械球磨法(1、干法[16],2、湿法[17]);(b)物理气相沉积[19];(c)化学气相沉积(插图为AFM 图像)[20];(d)共沉淀法[22];(e)水热法[24];(f)溶剂热法[26];(g)热分解法[28];(h)溶胶-凝胶法[30];(i)微乳液法[31];(j)声化学法[33];(k)电沉积法[34];(l)微生物合成法[35];(m)植物合成法[37];(n)仿生合成法[38]

    Figure  1.  SEM or TEM images of Fe3O4 nanomaterials obtained by different preparation methods (a) Mechanical ball milling (1, dry[16], 2, wet[17]); (b) Physical vapor deposition[19]; (c) Chemical vapor deposition(AFM image in the inset)[20]; (d) Co-precipitation[22]; (e) Hydrothermal[24]; (f) Solvent-thermal[26]; (g) Thermal decomposition[28]; (h) Sol-gel[30]; (i) Microemulsion[31]; (j) Acoustic chemical[33]; (k) electrodeposition[34]; (l) microbial synthesis[35]; (m) phytosynthesis[37]; (n) biomimetic synthesis[38]

    图  2  (a)Al2O3上Fe3O4材料示意图[20];(b)黑色区域为Fe3O4纳米材料,棕色区域为活性污泥[25];(c) 聚醇法制备示意图[27];(d)溶胶-凝胶爆炸辅助法制备Fe3O4纳米材料的机理[30];(e)多相分段流动反应合成过程示意图[31];(f)微乳液法合成Fe3O4纳米材料(W/O)[32];(g)超声合成Fe3O4[33];(h)异质结构前驱体Fe3O4/FexSy的合成过程示意图[34];(i)传统合成与仿生合成Fe3O4NPs[38]

    Figure  2.  (a) Schematic diagram of Fe3O4 film on Al2O3[20]; (b) black area is Fe3O4 nanoparticles and brown area is activated sludge[25]; (c) Schematic diagram of the preparation by the polyol method[27]; (d) Mechanism of Fe3O4 nanoparticles prepared by the sol-gel explosion-assisted method[30]; (e) Schematic diagram of the synthesis process of multiphase segmented flow reaction [31]; (f) Synthesis of Fe3O4 nanoparticles (W/O) by the microemulsion method[32];(g ) synthesis of Fe3O4 by ultrasound[33]; (h) schematic of the synthesis process of the heterostructured precursor Fe3O4/FexSy[34]; (i) conventional synthesis and biomimetic synthesis of Fe3O4NPs[38]

    图  3  (a) Fe3O4球体与Fe3O4/POA核壳球体的TEM图像[39];(b) Fe3O4/CS@Ag磁性材料的制备及SMSPE-SERS从预处理到检测过程示意图[40];(c) PAQR/Fe3O4复合纳米材料的合成过程[41];(d) Fe3O4@SiO2的合成工艺[43];(e) Fe3O4@Bi2S3的合成过程[47];(f) Au-Fe3O4纳米材料合成过程示意图[49];(g)以有机原料为基础的一步和两步AC制备示意图[50];(h) Fe3O4@CNTs示意图[51];(i) Cu-MOF和Cu-MOF@Fe3O4的合成流程示意图[53];(j)核壳结构 FPy-COF@PDA@Fe3O4 纳米球的合成流程示意图[54];(k) COF基纳米复合材料的合成工艺[55]

    Figure  3.  (a) TEM images of Fe3O4 spheres and Fe3O4/POA core-shell spheres[39]; (b) preparation of Fe3O4/CS@Ag magnetic microspheres and schematic diagram of the process of SMSPE-SERS from pretreatment to detection[40]; (c) synthesis process of PAQR/ Fe3O4 nanocomposites[41]; (d) synthesis process of Fe3O4@SiO2[43]; (e) synthesis process of Fe3O4 @Bi2S3 synthesis process[47]; (f) Schematic of the synthesis process of Au- Fe3O4 nanoparticles[49]; (g) Schematic of one-step and two-step AC preparations based on organic feedstocks[50]; (h) Schematic of Fe3O4@CNTs[51]; (i) Schematic of the synthesis process of Cu-MOF and Cu-MOF@ Fe3O4[53]; and (j) Schematic of the nucleoshell structure FPy-COF@PDA@ Fe3O4 nanorods[54]; (k) Schematic flow of the synthesis of COF-based nanocomposites[55]

    图  4  (a) Fe3O4MNPs的吸附效率与时间的关系[56];(b)外加磁场下BF染料在Fe3O4@Cd磁性微球吸附剂上的吸附−解吸过程[57];(c)亚甲基蓝、亚甲基绿和罗丹明B的分子吸收光谱[58];(d)不同因素对Fe3O4/Ti3C2纳米复合材料去除MG的影响[59];(e) Fe3O4NPs和Fe3O4/TiO2NCs在阳光直射下对MB的降解效果[60];(f) rGO/Fe3O4/ZnSe纳米催化剂降解MB[61];(g) rGO/Fe3O4/ZnSe纳米催化剂降解RB和MO[61];(h) Fe3O4/CuO投加量与COD去除率的关系[62];(i) MB吸光度分析[63]

    Figure  4.  (a) Adsorption efficiency of Fe3O4MNPs versus time[56]; (b) Adsorption-desorption process of BF dye on Fe3O4@Cd magnetic microsphere adsorbent under applied magnetic field[57]; (c) Molecular absorption spectra of methylene blue, methylene green and rhodamine B[58]; (d) Effect of different factors on the removal of MG by Fe3O4/Ti3C2 nanocomposites MB under direct sunlight[59]; (e) degradation of MB by Fe3O4NPs and Fe3O4/TiO2NCs under direct sunlight[60]; (f) degradation of MB by rGO/ Fe3O4/ZnSe nanocatalysts[61]; (g) degradation of RB and MO by rGO/ Fe3O4/ZnSe nanocatalysts[61]; (h) relationship between Fe3O4/CuO dosage and COD removal[62]; and (i) adsorption of MB by Photometric analysis[63]

    表  1  各种制备方法优缺点

    Table  1.   Advantages and disadvantages of various preparation methods

    Production method Raw materials Reaction
    Temperature /°C
    Reaction
    time
    Solvent Particle size/nm Advantages Disadvantages References
    Mechanical ball milling shot (in shotgun) Room temperature
    (RT)
    <20H H2O 11.1 Simple operation Easy to introduce impurities, not suitable for the preparation of different morphology of Fe3O4 nanocrystals [16][17]
    Physical vapor deposition Fe3O4、Si/MgO RT-500 / / 34-54 High purity, controllable, high efficiency Expensive equipment, high energy consumption, harsh reaction conditions [18]
    Chemical Vapor Deposition Fe(acac)3, MeOH 400 / / 110 High efficiency, easy to control Complex reaction process, requiring specific gases and reagents [20][21]
    Precipitation FeCl3·6H2O,
    FeSO4·7H2O
    60 2H H2O/
    EtOH
    10-32 Easy to implement, less hazardous Wide grain size distribution, need to control the conditions accurately [22][23]
    Hydrothermal FeCl3·6H2O,TEA 180 2-8H H2O 11.8 Strong magnetism at high temperatures, high product purity, easy to operate, low contamination High energy consumption, long reaction time, high equipment requirements [24]
    Solvent Thermal Method FeCl3·6H2O 200 4H EG 10-150 High purity, controllable size,
    fast reaction speed
    Limited choice of solvents, high temperature and pressure conditions [25]
    Thermal decomposition Fe(acac)3 200-270 20-55 min Octadecene, Oleylamine, Dioctyl Ether 9-19 Uniformity of nanoparticles, high saturation magnetization rate Requires high temperature conditions, difficult to control the reaction process [28]
    Sol-gel method Fe(NO3)3 220-320 1H H2O 37.2-
    43.5
    Controllable size and morphology, high uniformity, low temperature preparation High operating technology requirements, high equipment costs [29]
    Microemulsion FeCl2,FeCl3,HCl RT-50 25 min NH4OH solution 10 Controlled nucleation and growth, effectively avoiding agglomeration between particles Low yield, high cost [31]
    Acoustic Chemistry Fe 60 15 min Na2SO4 solution 50 Easier to achieve uniform mixing of media, high reaction rate Sensitive to reaction conditions, high energy consumption [33]
    Electrodeposition FeSO4·7H2O,Na2S2O3 RT 5 min deoxygenated water / Good biocompatibility Slower growth rate, high operation technology requirements [34]
    Microbial synthesis Fe2(SO4)3、S2 strain RT 5H H2O 20-70 Environmentally friendly, good biocompatibility, sustainability Long production cycle, low product purity, difficult to control [35]
    Phytosynthesis Fe(NO3)·9H2O、Natural tannins (green tea) / / / 23.4 Environmentally friendly, good biocompatibility, resourcefulness Complex extraction process, low product purity, difficult to control [36]
    Biomimetic synthesis FeSO4·7H2O、KOH、KNO3、Mms6-28 RT-90 -5H / / Controlled particle size, environmentally friendly, structural complexity Higher cost, more demanding reaction conditions [38]
    下载: 导出CSV

    表  2  Fe3O4纳米材料最大吸附量的比较

    Table  2.   Comparison of maximum adsorption capacity of Fe3O4 nanomaterials

    AdsorbentDyeDye amount/
    (mg·g−1)
    Adsorbent amountTemperaturePHTime/minAdsorption capacity/(mg·g−1)Removal/
    adsorption rate
    Fe3O4(Elham Ghoohestan)MB120.5 mg/mLRT7.56017.7989%
    Fe3O4@CdBF25100 mgRT76023.5>95%
    Fe3O4
    (Hoang Anh Thid)
    MB50020 mg/
    25 mL
    RT790268.64~97%
    Fe3O4/Ti3C2MG105 mgIncreased removal rate at higher temperaturesIncreased
    removal rate at
    elevated pH
    604.6899%(100 mg of adsorbent)
    Notes: MB: Methylene Blue; BF: Basic Fuchsin; MG: Malachite Green.
    下载: 导出CSV
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出版历程
  • 收稿日期:  2024-07-30
  • 修回日期:  2024-09-25
  • 录用日期:  2024-10-14
  • 网络出版日期:  2024-10-29

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