多酚改性纤维增强聚合物基复合材料研究进展

方策; 宋立健; 丁玉梅; 谭晶; 杨卫民; 程礼盛

doi:10.13801/j.cnki.fhclxb.20230413.001

多酚改性纤维增强聚合物基复合材料研究进展

doi: 10.13801/j.cnki.fhclxb.20230413.001

方策¹,
宋立健^{1, 3},
丁玉梅¹,
谭晶¹,
杨卫民^{1, 2},
程礼盛^{1, 2, ,}

1.
北京化工大学　机电工程学院，北京 100029
2.
北京化工大学　有机无机复合材料国家重点实验室，北京 100029
3.
中国石化　北京化工研究院，北京 100013

基金项目: 国家自然科学基金 (52073012)

详细信息

通讯作者:
程礼盛，博士，副教授，硕士生导师，研究方向为高分子材料先进制造　E-mail: chengls@mail.buct.edu.cn

中图分类号: TB332
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- 被引次数: 0
出版历程
- 收稿日期: 2023-02-22
- 修回日期: 2023-03-23
- 录用日期: 2023-04-05
- 网络出版日期: 2023-04-14
- 刊出日期: 2023-10-15

Research progress on polyphenols modified fiber reinforced polymer composites

FANG Ce¹,
SONG Lijian^{1, 3},
DING Yumei¹,
TAN Jing¹,
YANG Weimin^{1, 2},
CHENG Lisheng^{1, 2
, ,}

1.
College of Mechanical and Electrical Engineering, Beijing University of Chemical Technology, Beijing 100029, China
2.
State Key Laboratory of Organic-Inorganic Composites, Beijing University of Chemical Technology, Beijing 100029, China
3.
Beijing Research Institute of Chemical Industry, Sinopec Corporation, Beijing 100013, China

Funds: National Natural Science Foundation of China (52073012)

摘要

摘要: 多酚是一种含有多个酚羟基的化合物，广泛存在于天然植物中。多酚中含有大量疏水芳香环和酚羟基，与材料之间能够实现氢键、金属配位和π-π相互作用等多种类型的相互作用，被广泛应用于材料功能化改性中。本文综述了多巴胺、邻苯二酚、没食子酸及单宁酸4种多酚在纤维增强聚合物基复合材料改性方面的研究进展，其中主要包括不同多酚的结构及特性、对纤维表面的改性方法及在纤维增强聚合物基复合材料中的应用；最后，结合目前多酚的应用和限制，对多酚改性研究的未来研究方向和研究重点进行了展望。
- 纤维增强聚合物基复合材料 /
- 改性方法 /
- 多巴胺 /
- 邻苯二酚 /
- 没食子酸 /
- 单宁酸
Abstract: Polyphenols are compounds with abundant phenolic hydroxyl groups which can be widely found in natural plants. Polyphenols can interact with the various materials to form hydrogen bonds, metal coordination and π-π interactions. Over the past few years, polyphenols have been widely applied in material functional modifications. In this paper, the structures and properties of polyphenols, including dopamine, catechol, gallic acid and tannic acid were reviewed. Meanwhile, the modification methods of fiber surface and the applications of fiber reinforced polymer composites were introduced. Finally, a prospective analysis on the future research direction and focus of polyphenol modification studies were provided.
- fiber reinforced polymer composites /
- method of modification /
- dopamine /
- catechol /
- gallic acid /
- tannic acid

HTML全文

图 1 多酚结构：(a) 邻苯二酚(CL)；(b) 多巴胺(DA)；(c) 没食子酸(GA)；(d) 单宁酸(TA)

Figure 1. Structure of polyphenols: (a) Catechol (CL); (b) Dopamine (DA); (c) Gallic acid (GA); (d) Tannic acid (TA)

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图 2 多酚与其他材料之间的相互作用^[33]

Figure 2. Various interactions between polyphenols with different materials^[33]

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图 3 在碳纤维(CF)上制作“砖混”结构示意图^[43]

Figure 3. Schematic illustration of fabrication of brick-and-mortar wall on the carbon fiber (CF)^[43]

PDA—Polydopamine; PNi—Polydopamine-Ni(OH)₂

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图 4 (a) CF共沉积处理工艺示意图；(b) 不同复合材料的界面剪切强度(IFSS)；(c) CF复合材料的界面增强机制 ^[57]

Figure 4. (a) Schematic illustration of co-deposition treatment procedure of CF; (b) Interfacial shear strength (IFSS) of different composites; (c) Interfacial enhancement mechanism of CF composites^[57]

APTES—Aminopropyltriethoxysilane

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图 5 超高分子量聚乙烯(UHMWPE)纤维的TA表面改性工艺图^[61]

Figure 5. Scheme diagram of TA surface modification to ultra high molecular weight polyethylene (UHMWPE) fiber^[61]

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图 6 碳纤维增强复合材料(CFRP)断口表面的SEM图像：(a) 原始 CF/RPU 复合材料；(b) (CF-Ni)/RPU 复合材料；((c), (d)) (CF-TA-Ni)/RPU 复合材料^[67]

Figure 6. SEM images of the carbon fibre reinforced polymer (CFRP) fractured surface: (a) Pristine CF/RPU composites; (b) (CF-Ni)/RPU composites; ((c), (d)) (CF-TA-Ni)/RPU composites^[67]

RPU—Rigid polyurethane

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图 7 (a) TA混合物2 h内颜色变化；(b) 混合物的紫外吸收光谱^[76]

Figure 7. (a) Color change of TA mixed solution before and after 2 h; (b) UV absorption spectra for the mixtures^[76]

DPPH—2, 2-diphenyl-1-picrylhydrazyl; BA—Boric acid; MEL—Melamine

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图 8 垂直燃烧试验中对CFRP施加火焰10 s点燃后不同时间的代表性图像^[80]

Figure 8. Images during vertical burning test at different time of flame applied for 10 s to CFRP samples for ignition^[80]

DGEBA—Diglycidyl ether bisphenol A

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表 1 多酚对纤维改性处理

Table 1. Fiber modification by polyphenols

Fiber	Matrix	Main compositions of coating	Performance	Ref.
Carbon fiber	Epoxy	GA, gelatin	IFSS: 85.6 MPa; Surface energy of the substrate (γ^P): 75.41 mN/m	[34]
Polyester fiber	None	GA, EDA	Water contact angle reduced by 57.2°; The tensile strength of the modified fiber paper (2.022 kN/m) were increased by 35.2%	[35]
Carbon fiber	PI	PDA, Fe³⁺ minerali- zation (β-FeOOH)	Tensile strength: 202.5 MPa; Tensile modulus: 7.445 GPa; Low wear rates under different sliding speed (5 N, 200-500 r/min, 60 min)	[36]
Carbon fiber	Nanosilica epoxy	PDA	After the 3-week salt spray test, the ILSS value of the PDA-SiO₂ CFRP laminate is still 11% higher than that of the unmodified CFRP	[37]
Glass fiber	None	PDA, Ag NPs	Conductivity: 2.49×10⁶ S/m; Great flexibility (Could easily operate as a conductive wire for a LED light even under various bending angles)	[38]
UHMWPE fiber	Rubber	CL, TEPA, ZnO NPs	Water contact angle: 36.2°; Surface energy: 37.8 mJ/m²; Pull-out force: 32.3 N	[39]
PET fiber	Epoxy	CL, PEI	Water contact angle: 58.9°; The fabric melting temperature and decomposition temperature increased from 253.78℃ and 394.08℃ to 255.01℃ and 398.21℃, respectively	[40]
Polyamides fiber	None	TA/Thiophene	Conductivity: 45 kΩ/cm; Electrothermal performance (Within 75 s, the temperature rises from 26.8 to 29.1℃ and basically reaches a robust level)	[41]
Wood fiber	None	TA, Fe(II) ions	Surface area is increased 66.8% by TA; The complexes promote the pyrolysis of wood fibers at lower temperature (162℃) and generate more residual char (110%)	[42]
Notes: UHMWPE—Ultra high molecular weight polyethylene; PET—Polyethylene glycol terephthalate; EDA—Ethylenediamine; PI—Polyimide; PDA—Polydopamine; GA—Gallic acid; CL—Catechol; TEPA—Tetraethylenepentamine; PEI—Polyethyleneimine; TA—Tannic acid; IFSS—Interfacial shear strength; NPs—Nanoparticles; ILSS—Interlaminar shear strength; CFRP—Carbon fibre reinforced polymer.

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