T6热处理/高频脉冲电流处理下SiC/2009Al复合材料的组织演变及力学性能

Microstructural evolution and mechanical properties of SiC/2009Al composites under T6 heat treatment/high-frequency pulsed current treatment

  • 摘要: 对粉末冶金法+热挤压技术制备的30vol.% SiC/2009Al复合材料进行T6热处理和高频脉冲电流处理,对两种状态下复合材料的微观组织演变差异进行分析,并对复合材料的微纳力学行为、拉伸力学性能进行测试。研究结果表明:挤压态复合材料内部晶粒被严重拉长变形,内部弥散分布Al2Cu和Mg2Si析出相。喷丸变形后,复合材料表面在发生变形的同时产生了一定数量的微裂纹。喷丸态复合材料内部存在高位错密度及应变强化;在T6热处理后,Al基体区域部分发生静态回复,小角度晶界占比由喷丸态的42.0%降低至17.2%;高频脉冲电流处理后,复合材料表面发生更高比例的静态回复再结晶,小角度晶界占比由喷丸态的42.0%降低至11.9%。高频趋肤和邻近效应有效去除了复合材料的宏/微观残余应力,其表面区域的KAM数值由喷丸态的0.66降低至0.29。10000 Hz电流处理态复合材料的拉伸强度及延伸率可达456 MPa和19.5%,较喷丸态分别提高38.6%和29.14%,被证实为一种更为优异的后处理强化技术。

     

    Abstract: 30vol.% SiC/2009Al composites fabricated by powder metallurgy combined with hot extrusion technology were subjected to T6 heat treatment and high-frequency pulsed current treatment. The differences in microstructural evolution of the composites under these two conditions were analyzed, and the nano-mechanical behavior and tensile mechanical properties of the composites were tested.The results show that the internal grains of the as-extruded composites are severely elongated and deformed, with Al2Cu and Mg2Si precipitated phases dispersedly distributed inside. After shot peening deformation, the composite surface undergoes deformation while generating a certain number of microcracks. High dislocation density and strain hardening exist inside the shot-peened composites; after T6 heat treatment, partial static recovery occurs in the Al matrix region, and the proportion of low-angle grain boundaries decreases from 42.0% (shot-peened state) to 17.2%. After high-frequency pulsed current treatment, a higher proportion of static recovery and recrystallization occurs on the composite surface, and the proportion of low-angle grain boundaries decreases from 42.0% (shot-peened state) to 11.9%.The high-frequency skin effect and proximity effect effectively eliminate the macro/micro residual stress of the composites, and the KAM (Kernel Average Misorientation) value in the surface region decreases from 0.66 (shot-peened state) to 0.29. The tensile strength and elongation of the composites treated with 10000 Hz current reach 456 MPa and 19.5%, which are 38.6% and 29.14% higher than those of the shot-peened state, respectively. This confirms that high-frequency pulsed current treatment is a more excellent post-treatment strengthening technology.

     

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