C/SiC壁板的制备层间缺陷特点及性能分析

Characteristics and Performance Analysis of Interlayer Defects in the Preparation of C/SiC Panel

  • 摘要: 针对C/SiC复合材料壁板制备环节常见的分层开裂情况,选择树脂转移浸渍裂解(RTIP)成型/致密化工艺的产品为对象进行了特征和性能分析。对分层形貌进行观测认为,制备前期和复合后期的层间缺陷分别具有碳纤维束之间分层和碳纤维束内部开裂的两种不同特征。切割制备出C/SiC的无缺陷试验件、以及不同特征下具有不同层间缺陷尺度的试验件,开展强度性能测试。Ⅰ型、Ⅱ型层间断裂韧性试验均未产生层间裂纹尖端扩展的现象和数据特征,推断这种层间缺陷的裂纹尖端扩展阻力要明显大于标准试验采用的机加制备开缝情况。进一步进行了面内拉伸、面内压缩性能测试,分析了材料性能衰减的机制并由试验数据拟合得出与层间缺陷尺度之间的规律。为了在体现试验件整体损伤形貌的同时表征到层间缺陷区域的材料细节特征,采用了在缺陷近场细观形貌构造、远场宏观等效并在两者之间区域逐级过渡连接的宏/细观一体化多尺度数值建模和分析方法。计算的应力场特点进一步验证了试验判断的合理性。

     

    Abstract: In view of the common delamination cracking in the preparation of C/SiC composite panel, the characteristics and properties of the products produced by resintransfer infiltration pyrolysis (RTIP) molding/densification process were analyzed. The observation of delamination morphology shows that the interlayer defects in the early stage of preparation and the late stage of composite have two different characteristics: delamination between carbon fiber bundles and internal cracking of carbon fiber bundles.Non-defective specimens of C/SiC and specimens with different interlaminar defect scales under different characteristics were cut and prepared, and the strength performance were tested. The mode-Ⅰ and mode-Ⅱ interlaminar fracture toughness tests did not produce the phenomenon and data characteristics of interlayer crack tip propagation, so it is inferred that the interlayer tip propagation resistance of these defect is obviously greater than that of machining cracks used in standard tests. Furthermore, in-plane tensile and in-plane compressive tests were carried out, and the mechanism of material properties attenuation was analyzed, and the law between the material properties and interlayer defect scales was obtained by fitting the experimental data. In order to represent the overall damage morphology of the specimen and the material details of the interlayer defect region, a multi-scale macro-meso integrated numerical modeling method was adopted, which is composed of meso-morphology structure near the defect, macro-equivalence in the distance and the gradual transition connection between the two regions. The characteristics of the calculated stress field further verify the rationality of the experimental analysis.

     

/

返回文章
返回