WC、ZrO2 、Cr2O3 和Al2O3 陶瓷颗粒/ 镍合金复合涂层微观组织结构的分形

FRACTAL CHARACTERISTIC OF MICROSTRUCTURE OF WC, ZrO2, Cr2O3AND Al2O3 CERAMIC PARTICLES/ NICKEL ALLOY COMPOSITE COATINGS

  • 摘要: 采用等离子喷涂工艺, 制备了WC、ZrO2 、Cr2O3 和Al2O3 陶瓷颗粒/ 镍合金复合涂层。用X 射线衍射研究了陶瓷颗粒复合涂层相的分布; 用里氏硬度计测量陶瓷颗粒/ 镍合金复合涂层的硬度; 用CSS-1110 电子万能试验机研究陶瓷颗粒复合涂层的弯曲断裂性能。对涂层金相组织结构进行二值化处理, 利用Sandbox 法对陶瓷颗粒在金属基体中的分布进行研究, 得到了不同体积分数下陶瓷颗粒复合材料涂层的分维数。结果表明,陶瓷颗粒/ 镍合金复合涂层分维数随陶瓷颗粒含量的增加而增加, 与陶瓷颗粒种类无关; 陶瓷颗粒/ 镍合金复合涂层硬度和分维数随陶瓷颗粒直径减小而增加。随着分维数的增加, 复合涂层弯曲断裂角下降。

     

    Abstract: Four kinds of WC, ZrO2, Cr2O3 and Al2O3 ceramic particles/ nickel alloy composite coatings were prepared with the plasma spraying method. The X-ray diff raction analysis was used to investigate the phase constituentof ceramic particles in composite coatings. The hardness of the ceramic particles/ nickel alloy composite coating wasmeasured by the Leeb hardness tester. The properties of bend breaking of composite coatings were measured usingCSS-1110 elect ric all-purpose test meter. The micro-st ructures of composite coatings were t reated as a binarizationaf ter morphological processing. The f ractal dimensions of the ceramic particles/ nickel alloy composite coatings withdifferent volume f ractions of particles were obtained by means of the Sandbox method. Experimental result s indicatethat the dist ributions of ceramic particles in metal mat rix have a f ractal characteristic. The f ractal dimensions increase with the increase of particle volume f ractions. The dimensions are irrelative with the kinds of ceramic particles. The hardness and dimension of composite coatings increase with the decrease of diameter of ceramic particles.The bending f racture angles decrease with the increase of dimensions of ceramic particles/ nickel alloy compositecoatings.

     

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