Microstructural characteristics and thermal shock resistance ofnano-powder reinforcing cermets
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摘要: 为了进一步提高金属陶瓷的力学性能及其刀具的高速切削性能, 研究了纳米增强金属陶瓷的显微组织特征和热冲击性能。扫描电镜和透射电镜分析表明: 组织中陶瓷相呈现典型的芯2壳结构特征; 芯为TiC 或Ti (C ,N) , 而壳则为( Ti ,Mo ,W) (C ,N) 固溶体。纳米增强金属陶瓷机制为细晶强化、弥散强化和固溶强化。热冲击实验表明: 随着热循环的进行, 材料中孔洞的数量、孔洞的尺寸以及微裂纹的尺寸随之增大; 同时, 热循环过程中出现的表面氧化、裂纹长大、偏转以及桥接现象也很显著。与常规Ti (C ,N) 金属陶瓷相比, 纳米增强金属陶瓷的抗热冲击性能明显提高。Abstract: Microst ructural characteristics and thermal shock resistance of nano-powder reinforcing Ti (C ,N) basedcermet s were investigated in order to efficiently improve the mechanical properties of Ti (C ,N) based cermet s and thehigh-speed cutting behaviors of cermet s cutters. SEM and TEM analyses show that the coarser ceramic particles exhibit a typical core-rim st ructure (core is usually referred to as TiC or Ti (C ,N) and rim is virtually a ( Ti ,Mo ,W)(C ,N) solid solution) . The nano-powder reinforcing mechanisms can be summarized as grain fining st rengthening ,dispersion st rengthening and solid solution st rengthening. The thermal shock test s on nano - powder reinforcingcermet s and conventional cermet s show that the quantity and size of the voids plus the size of micro-cracks in bothcermet s increase and other phenomena such as surface oxidation , cracks growth , cracks deflection and cracks bridging are found to become increasingly apparent with thermal shock cycles , and the nano-powder reinforcing cermet spossess a better thermal shock resistance in comparison with conventional cermet s.
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Key words:
- nano-powder reinforcing cermets /
- microst ructure /
- thermal shock resistance /
- voids
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