Abstract:
Magnetic activate carbon (MAC) coupled by chitosan-glutaraldehyde crosslinking technique was synthesized by ferric salts chemical precipitation method using activate carbon as raw meterial. Based on MAC, Br-N codoped TiO
2/magnetic carbon composites (Br
x-N-TiO
2/MAC) were prepared by a facile sol-gel method.The synthesized composites were characterized by XRD, UV-Vis diffuse reflectance spectroscopy (DRS), N
2 adsorption-desorption test (BET), SEM and XPS. The photocatalytic activity of the composites was evaluated by photocatalytic degradation of salicylic acid under visible light irradiation. Compared with N-TiO
2/MAC, Br
x-N-TiO
2/MAC has a better photocatalytic performance. The degradation effect of Br
0.35-N-TiO
2/MAC to salicylic acid is the best, and the photocatalytic degradation rate of Br
0.35-N-TiO
2/MAC for 3 h can reach up to 83% after 1 h dark absorption. High concentration of salicylic acid can inhibit the photocatalytic reaction rate of Br
x-N-TiO
2/MAC. After reused for three times, the removal rate of Br
0.35-N-TiO
2/MAC to salicylic acid can still reach 78%, which proves the composites have a good chemical stability.