Aging behavior of sub-micron Al2O3P/Al-Mg-Si composites
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摘要: 为了研究亚微米级Al2O3颗粒对基体合金时效过程的影响规律,在 6061 铝合金基础上调整Mg、Si含量,采用压力浸渗法,制备了Al2O3体积分数为30%的亚微米级Al2O3P/Al-2.26Mg-0.63Si复合材料。通过硬度试验、SEM和TEM等手段,研究了复合材料及其基体合金的时效行为。结果表明,Al-2. 26Mg-0.63Si 合金的时效过程比较明显,随时效温度的提高峰时效时间提前,190℃时出现时效软化现象。亚微米Al2O3颗粒的加入强烈抑制复合材料的时效过程,时效曲线未出现明显时效峰。分析认为,由于大部分Mg 元素被消耗在界面形成MgAl2O4,且基体中位错稀少,不利于溶质原子扩散,因此复合材料中沉淀相在过时效阶段仍停留在GP区状态,没有充分长大,时效析出受到抑制。
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关键词:
- 亚微米Al2O3颗粒 /
- Al-Mg-Si /
- 复合材料 /
- 时效 /
- 界面
Abstract: 30 vol%Al2O3P/Al-2.26Mg-0.63Si composite was fabricated by the Pressure Infiltration Method for investigating the aging behavior of the composites with sub-micron Al2O3 particles. The corresponding matrix alloy was obtained by tailoring the Mg and Si contents of 6061Al. The aging behaviors of the composites and the corresponding matrix alloy were investigated by means of Brinell hardness test,SEM and TEM. The results show that the aging behavior of the matrix alloy of Al-2.26Mg-0.63Si is visible and the peak-aging time is put ahead with the aging temperature rise. The aging softening phenomenon appears at 190℃. The addition of sub-micron Al2O3 particles rest rains strongly the precipitation process within the matrix. There are no obvious aging peaks to appear in the aging-hardening curves of the composites. TEM observation shows that a mass of MgAl2O4 spinel forms in the interfaces , and atoms cannot diffuse efficiently for little dislocations existing in the matrix alloy. Therefore,GP zone does not grow-up at over-aged course within the composites,and the aging precipitation is restrained.-
Key words:
- sub-micron Al2O3 /
- Al-Mg-Si alloy /
- composites /
- aging /
- interface
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