FANG Jinghua, XIANG Jinzhong, HU Yongmao, et al. PREPARATION OF NANOCRYSTALLINE(Ni,Zn)Fe2O4 COMPOSITE MATERIAL WITH COPRECIPITATION AND ITS CHARACTERISTICS1[J]. Acta Materiae Compositae Sinica, 2004, 21(1): 12-16.
Citation: FANG Jinghua, XIANG Jinzhong, HU Yongmao, et al. PREPARATION OF NANOCRYSTALLINE(Ni,Zn)Fe2O4 COMPOSITE MATERIAL WITH COPRECIPITATION AND ITS CHARACTERISTICS1[J]. Acta Materiae Compositae Sinica, 2004, 21(1): 12-16.

PREPARATION OF NANOCRYSTALLINE(Ni,Zn)Fe2O4 COMPOSITE MATERIAL WITH COPRECIPITATION AND ITS CHARACTERISTICS1

  • Received Date: 2002-11-12
  • Rev Recd Date: 2003-03-23
  • Publish Date: 2004-02-15
  • By using FeSO4·7H2O, NiSO4·6H2O and ZnSO4·7H2O as raw materials, with a coprecipitation method, the basic carbonate precursor containing very fine crystalline grain is first synthesized and then nanocrystalline (Ni,Zn)Fe2O4 composite particles followed by sintering for one hour can be obtained. The microstructure was measured by using XRD and TEM. And then, the infrared absorption and gas-sensitization of the samples have been investigated. The results show that the diameter of the nano-particles is about 50nm at 800℃.

     

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      沈阳化工大学材料科学与工程学院 沈阳 110142

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