Preparation and characterization of NiCo/ PTFE magnetic composite membrane
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Abstract
On the basis of template and elect roless methods , NiCo/ PTFE magnetic composite membranes were prepared with N2H4 as reducing agent . The paper studied the optimum preparation conditions and characterized st ructures and magnetic properties of the membranes by DSC , SEM , XRD , VSM. The result s show that magnetic composite membranes with susceptibility of 0. 16 cm3 / g have ferromagnetic property (Ms = 83. 38 Am2 / kg , Mr = 29. 31Am2 / kg , Hc = 111. 47 Oe) , which are obtained f rom solution of 0. 14 mol/ L Co2+ , 0. 06 mol/ L Ni2+ , 1. 00 mol/ LNaOH , 0140 mol/ L N2H4 at 70 ℃and 70 min. Magnetic Ni and Co particles appear in the pores and on the surfaceof PTFE membranes , and no chemical bonds are found between magnetic particles and membranes. The compositemembranes have int rinsic properties of sof t magnetic material.
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