Abstract: A new fabrication process on Fe₃Al/Al₂O₃ composite has been researched. This is important not only to produce Fe₃Al/Al₂O₃ composite by sintering process that does not employ pressure to composite, but also to open up and use this composite. This new fabrication process can be called melting & casting sintering process (MCSP). MCSP has proved to be a good desirable way by experimental study.